Qualitative Determination of Proanthocyanidin Cleavage Products After Acid-Catalyzed Degradation in the Presence of Excess Phloroglucinol by Cyclodextrin-Modified Micellar Electrokinetic Chromatography
نویسندگان
چکیده
A micellar electrokinetic chromatographic (MEKC) method has been established for the identification and determination of acid-catalyzed proanthocyanidin cleavage products in the presence of phloroglucinol. Using fused-silica capillaries (50=57 cm, 22 kV) with phosphate buffer containing sodium dodecyl sulfate as the surfactant and b-cyclodextrin as modifier, structurally similar phloroglucinol adducts and flavan-3-ols were fully separated.
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